Institute of Materials Processing
at Michigan Tech		 Electron microscope
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Laboratories List

The advantages of Michigan Tech's Institute of Materials Processing is that it has a large selection of equipment that can be drawn from to set up a customized pilot plant test circuit.

1. MATERIAL CHARACTERIZATION

    A. Optical microscope and mount preparation
    • 1 Nikon HFX-11A polarized microscope with photograph and image analysis capabilities
    • 1 Nikon epiphot metallographic microscope with photograph and image analysis capabilities
    • 1 Leitz Ortholux microscope and camera
    • 2 Nikon SMZ-2T stereo microscopes
    • 1 Bausch & Lomb stereozoom & microscope
    • 1 complete sample mounting, sectioning, and polishing laboratory
    • 1 Darkroom and related photo equipment
    B. Electron microscope, electron microprobe, and x-ray
    • 1 JEOL JSM 820 SEM, with EDS (including light elements) and Tracor Northern image analysis system
    • 1 JEOL 8600 Superprobe with WDS, EDS, SEM, and image analysis capabilities (Met)
    • 1 Radioisotope energy dispersive x-ray fluorescence system (Met)
    • 1 Computer-controlled x-ray fluorescence spectrometer with automatic sample changer (Met)
    • 1 JEOL 100CX STEM (Met)
    • 1 Phillips 301 TEM (Met)
    • 1 Scanning auger microprobe (Met)
    • 1 Siemens MRS 300 x-ray fluorescence spectrometer
    • 4 automated x-ray diffractometer (Met)
    • 1 Ladd vacuum evaporation unit
    • 1 Anatech Hummber VII sputter
    C. Particle Size
    • 1 Microtrac particle size analyzer, Leed & Northrup Microtrac II
    • 1 Sedigraph particle size analyzer, Micromeritics 5000ET
    • 1 Coulter counter
    • 3 Rotaps with full range sieves
    • 1 Fisher sub-sieve sizer
    • 1 Aminco air classified roller particle size analyzer
    • 1 Federal air classifier
    • 1 Sonic sifter
    D. Surface, Volume, Density
    • 1 Zeta potential reader, Komline-Sanderson Model ZR-10
    • 1 BET apparatus, Micromeritics FlowSorb II 2300 with gas mixer
    • 1 Pycnometer, Micromeritics multivolume 1305
    • 1 Blaine tester
    • 1 Jolly specific gravity balance
    • 1 Coal washability and heavy liquid separation lab
    • 1 1" glass hydrocyclone and related equipment
    • 1 contact angle apparatus
    E. Viscosity, Permeability, Porosity, Turbidity and Others
    • 2 Brookfield viscometer
    • 1 Stormer viscometer
    • 1 FANN viscometer
    • 1 Du Nouy tensiometer
    • 1 Permeability measuring device
    • 1 Mercury intrusion porosimeter
    • 1 Thermal analysis system, see Chemical Analysis section
    • 2 Magnetic susceptibility meter, see Magnetic section
    • 1 Hellige turbidimeter
    F. Mechanical Properties
    • 1 Leco Rockwell hardness tester
    • 1 High-Vacuum tensile testing chamber (12"x12"x16", water-cooled) (Met)
    • 1 Sonntag Universal fatigue testing (+1 Kip, +0.375") (Met)
    • 1 22 Kip servo-hydraulic test machine (Met)
    • 1 30 Kip screw-driven test machine (Met)
    • 1 Instrumented impact tester
    • 1 Universal testing machine (120 Kip) (ME-EM)
    • 1 MTS sheet metal formability testing system (ME-EM)
    • 1 Instron universal testing (2 Kip) (ChE)
    • 1 Instron benchtop universal tester (200 lbs) (ChE)
    • 1 Instron universal tester (10 kip) (ChE)
    • 1 Tinius-Olsen screw-driven tester (120 Kip) (Civ.)
    • 1 22 Kip MTS servo-hydraulic tester (Civ.)
    • 1 Baldwin Model 300CT (300 Kip) tester (Civ. E)
    • 1 Leco Vickers/Knoop hardness tester (Met)
    • 1 Leco Rockwell hardness tester (Met)

2. CHEMICAL ANALYSIS

    • Fourier Transform Infrared Spectrometer, Perkin-Elmer 1600 with long path gas cell, diffuse reflectance, multiple internal reflectance, and variable angle specular reflectance accessories
    • Ultraviolet Spectrometer, Perkin-Elmer Lambda 3B with integrating sphere accessory
    • Raman spectrometer, Jobin-Yvon U1000 with optical microscope
    • Complete equipment for volumetric, gravimetric, titrimetric, colorimetric, electrolytic, and other types of analysis.
    • Carbon and sulfur analyzer (LECO CS-46 & SC 32)
    • Hydrogen determinator
    • Nitrogen determinator
    • pH meters
    • Muffle furnace, drying ovens
    • Adiabatic bomb calorimeter (Parr Model 1241)
    • Analytical balances
    • Atomic absorption spectrophotometer (PE Model 603) with hydride
    • generator and cold vapor mercury system
    • Graphite furnace (PE Model 2100)
    • Thermal analysis system (DuPont 2100)
    • Differential scanning calorimeter (DuPont Model 951)
    • Thermomechanical analyzer (DuPont Model 943)
    • Differential thermal analyzer (DuPont Model 1600 DTA)

3. THERMAL PROCESSING

    • 1 Vacuum Industries vacuum furnace, 10-6 torr, 8"x8"x20" hot zone, 1650°C, with glove box
    • 2 Rotating furnaces, 300-gram charge
    • 1 Rotating furnace, 500-lb charge
    • 1 Lindberg 1500°C tube furnace
    • 1 Leco tube furnace
    • 1 Globar tube furnace
    • 1 Linder apparatus
    • 1 Lucifer inert atmosphere box furnace, 12"x12"x12", 2150°F
    • 1 Lucifer, globar, muffle, 2800°F
    • 1 Lindberg - H.D., muffle, 2000°F
    • 1 plasma-arc furnace
    • 1 Marko melt spinner
    • 1 vacuum/air induction melter, 20 kw
    • 1 Centorr vacuum furnace for 2500°C (Met)
    • 1 Astro graphite vacuum/inert furnace for 3000°C (Met)

4. MICROWAVE PROCESSING

    • 1 Wavemat inert/air automated microwave sintering furnace, 2000°C
    • 1 microwave autoclave
    • 1 microwave oven
    • 1 microwave tube furnace

5. CHEMICAL PROCESSING

    • 1 Chemical processing lab with regular hoods and California hoods
    • 1 wet processing lab with hoods, ventilation systems and wet benches
    • 1 gas scrubbing system
    • 1 Ultrasonic nozzle deflocculating system
    • 1 spray dryer
    • 1 vacuum extraction/distillation system

6. CONSOLIDATION PROCESSING

    • 1 controlled atmosphere processing system, including solvent dryer, attritor, 25 ton press, slurry blender, pulverizer, canning system, residual gas analyzer (mass spectrometer), and vacuum furnace
    • 1 30T Spex sample press
    • 1 75 ksi Quick-HIP
    • 1 Insta-HIP, 150 ksi
    • 1 cold isostatic press, 100 ksi

7. FROTH FLOTATION PROCESSING

    • 1 Galigher cell, Model LA-500
    • 4 WEMCO cells, 600-1000 gm
    • 1 Denver D-1 machine, 1000 and 250 g glass bowls, tachometer
    • 1 Denver D-12 machine
    • 1 Denver cell, 500 gm
    • 1 WEMCO attrition machine, Model 5202FNOTX
    • 1 Deister flotation column
    • 3 MTU packed flotation column
    • Conditioners, rod mills, ball mills, pH meters, balances, binoc microscope, water deionizer and related equipment

8. GRAVITATIONAL PROCESSING

    • 2 jigs, Denver #1
    • 2 tables, Wilfley 13A
    • 2 hydraulic classifiers
    • 1 heavy liquid setup
    • 1 heavy media Ericson cone test unit
    • 1 Deister concentrating table No. 15-S
    • 1 Triple S air table
    • 3 air cyclone systems

9. MAGNETIC AND ELECTROSTATIC PROCESSING

    • 1 Eriez L-4-20 high intensity magnetic separator, 20,000 gauss
    • 1 Eriez L-4 high intensity magnetic, 8"
    • 1 Eriez Rare Earth Magnetic Roll Separator
    • 3 demagnetizing coils, 60, and 400 cycle
    • 2 Davis tubes
    • 1 Carpco wet high intensity magnetic separator
    • 1 Carpco dry high intensity magnetic separator
    • 1 Dings batch laboratory cobber, 9" drum
    • 1 Steffenson cobber, 3" drum
    • 1 Johnson Matthey magnetic susceptibility balance
    • 1 Satmagan magnetic balance
    • 1 Hall effect gauss meter
    • 1 Stearns crossbelt mag sep, 3" (Met)
    • 1 Eriez 50 kv electrostatic separator
    • 1 Carpco high tension separator, HP 16 (Met)
    • 1 Franz isodynamic separator (Met)

10. CONCRETE AND AGGREGATE

    • 1 Conrad freeze-thaw test unit, 8 cycles/24 hours
    • 1 sonometer with oscilloscope
    • 1 air entrained air meter
    • 1 slump measuring apparatus
    • 3 cement mixers
    • 1 Schmidt concrete test hammer
    • 1 controlled temperature and humidity room (CIV); related molds and tools relative to aggregate and concrete
    • 1 hydrosplit masonry cutter
    • See Mechanical Property section of material characterization for concrete testing

11. SAMPLE PREPARATION

    • 2 jaw crushers
    • 1 gyroll
    • 1 roll crusher
    • 2 pulverizers
    • 4 rotaps with full range of sieves
    • 2 blenders
    • 1 drying oven
    • 7 filter presses
    • Jones splitters and related equipment
    • 1 microwave oven, Model 403
    • 1 sieve shaker

12. GRINDING

    • Drais Perl mill, Model PM-1, 6TS-V
    • Bond grindability rod mill
    • Bond grindability ball mill
    • Spex mixer/mill
    • Rod and ball mills
    • Shatterbox pulverizer
    • Microtrac II, Leed & Northrup Model 7997-10, 0.70 to 700 microns

13. AGGLOMERATION

    • 1 extruding machine
    • 2 balling drums, 12" diameter
    • 2 green ball compression tests, Chatillon Model LTC
    • 1 Carver press compression testing machine
    • 1 motorized Dillon tester Model 6W-19
    • 1 tumble test drum - 3 ft.
    • 2 autoclave Cenco-Menzel, 350 psi, 2 gal. capacity
    • 1 autoclave Parr. 6000 psi, 1 liter capacity
    • 1 blender
    • 1 mix-muller, .2 ft3
    • 1 Cenco drying oven
    • Related materials testing devices

14. INJECTION MOLDING/EXTRUSION

    • 1 injection molder
    • 1 twin screw extruder
    • 1 hot blender
    • 1 granulator

15. CHEMICAL VAPOR DEPOSITION/THERMAL SPRAY

    • 1 microwave CVD system
    • 1 RF CVD system
    • 1 low pressure plasma spray system
    • 1 flame thermal spray system
    • 1 Raman spectrometer

16. MISCELLANEOUS EQUIPMENT

    • 1 machine shop with related equipment
    • 1 temperature regulated water bath and shakers
    • 1 ultrasonic bath
    • 1 ultrasonic dismembrator
    • 1 glove box
    • 1 Haake heating and cooling control system
    • 1 Stone effluent gas analysis (EGA) unit
    • 1 Bendix SO2 flame photometric monitor
    • 1 Bendix permeation system
    • Detailed information on other miscellaneous equipment such as ovens, pH meters, pumps, centrifuges, autoclaves, gas control units, geological and soil sampling devices, seismographs, corona dischargers, etc., are available upon request.

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